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    If you use a planetary ball mill, the manufacturer will usually offer grinding vessels that are adapted for vacuum and inert gas grinding. I've linked to just one example.

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    The average particle size FeTi powder to the air after ball milling in an inert gas of original FeTi is 45 /zm, which decreases to 16 mm atmosphere is effective for the improvement of the after 86 ks of milling.

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    Following milling, the powder is annealed under an inert gas flow at temperatures of 1400°C for six hours. The mechanism of this process is not known, but it is thought that the ball milling process forms nanotube nuclei, and the annealing process activates nanotube growth.

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    What is claimed is: 1. A method for preparing titanium nitride powder, which comprises subjecting mixed powder of titanium trichloride and lithium nitride to ball milling using a plurality of balls in an airtight reactor vessel under an inert gas atmosphere to form composite powder of titanium nitride and lithium chloride, and recovering the titanium nitride powder therefrom.

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